A novel metal complexes Cu (II), Co (II), Cd (II), Ru (III) from azo ligand 5-((2-(1H-indol-2-yl) ethyl) diazinyl)-2-aminophenol were synthesized by simple substitution of tryptamine with 2-aminophenol. Structures of all the newly synthesized compounds were characterized by FT IR, UV-Vis, Mass spectroscopyand elemental analysis. In addition measurements of magnetic moments, molar conductance and atomic absorption. Then study their thermal stability by using TGA and DSC curves. The DCS curve was used to calculate the thermodynamic parameters ΔH, ΔS and Δ G. Analytical information showed that all complexes achieve a metal:ligand ratio of [1:1]. In all complex examinations, the Ligand performs as a tridentate ligand, connecting Cu (
... Show Moreيهدف البحث الى دراسة تأثير ذكاء الاعمال بما يمتلكه من مقومات في تحقيق التنمية بهدف تحديد عناصر ذكاء الاعمال الاكثر تأثيرا في مجالات التنمية المستدامة للأقسام والشعب في وزارة العلوم والتكنولوجيا كونها منظمة تعمل على استخدام تكنولوجيا المعلومات وهي الاكثر تأثيرا في تطبيق ذكاء الاعمال. اعتمد ال على المنهج الوصفي والتحليلي للتعرف على مشكلة البحث وإثبات فرضياتها من خلال الربط النظري لمتغيراتها ، وبعد ذل
... Show MoreNew derivative molecular absorption spectrophotometric methods have been developed for the determination of Al (III) , Mn (II) , individually and binary mixtures . The aim of this model of study is to obtain analytical results characterized by adequate standard of analytical figures of merits through application of derivative Spectrophotometry (dnA/d?n). The two metals acetyl acetonates are chemically stable and are widely used as catalysts . Where Interferences are probable due to very close or nearby peaks or Summits, the Zero – Crossing derivative measurement technique is used to avoid interfering effects between two metals pairs.
كلية الفنون الجميلة بين تقادم المعرفة وعصر التحديات
ملخّص البحث
تكمن مشكلة البحث في الاكتشاف المبكر لسوء صحة الطلبة النفسية و محاولة ايجاد الحلول اللازمة لها في سنوات الدراسة الجامعية من حيث استخدام المواد الدراسية او اساليب التعامل او اسس العلاج الفردي المتبع من قبل الاساتذة مع الطلاب الذين يعانون من اي خلل نفسي او سلوكي، و ذلك لاهمية الحالة النفسية لمعلمي المستقبل و تاثير سلوكياتهم و انعكاسها على التدريس وعلى الطل
... Show MoreBackground: Direct measurement of intracellular magnesium using erythrocytes has been suggested as a sensitive indicator for the estimation of body magnesium store. Marked depletion in plasma and erythrocyte magnesium levels was particularly evident in diabetic patients with advanced retinopathy and poor diabetic control. While insulin has been shown to stimulate erythrocyte magnesium uptake, hyperglycemia per se suppressed intracellular magnesium in normal human red cells.
Aim of the study: To investigate the erythrocyte magnesium level in Iraqi type I and II diabetic patients, with specific emphasis on the effect of both, metabolic control and the type of antidiabetic treatments.
Methods: Sixty two diabetic patients (7 with type
Aspartate aminotransferase was purified from urine and serum of patients with type 2 diabetes in a 2 steps procedure involving dialysis bag and sephadex G-25 gel filtration (column chromatography). The enzyme was purified 346.23 fold with 1467% yield and 3.46 fold with 142.85% yield in urine and serum of patients with type 2 diabetes respectively. The purified enzyme showed single peak. The results of this study revealed that AST activity of type 2 diabetes urine and serum increased significantly (p<0.001) compared with control group.
The research includes the preparation of several complexes of the internal transition elements lanthanide (Ln = La, Nd, Er, Gd, and Dy) containing the 4f shell, with Schiff bases resulting from condensation reactions between 4-antipyrinecarboxaldehyde and 2-aminobenzothiazoles. Schiff's base was identified using FTIR spectra, UV-vis spectroscopy, elemental microanalysis CHNSO, nuclear magnetic resonance, mass spectrometry, and TGA thermal analysis. The complexes were studied and identified with elemental microanalysis CHNSO, FTIR spectroscopy, UV-vis spectroscopy, TGA thermal analysis, conductivity measurement, and magnetic sensitivity. The result showed that these complexes were classified as homogeneous bidentate complexes with th
... Show Moreهدف المقال الكشف عن تأثير استراتيجيات إدارة الموارد البشرية بأبعادها)استراتيجية األداء العالي، استراتيجية االلتزام العالي، استراتيجية االندماج العالي( في تحسين المعرفة الرقمية بأبعادها )االبداع والمبادرة، تكنولوجيا المعلومات، الموارد، المشاركة والتعاون، الجودة( في وزارة العلوم والتكنولوجيا. تم اختيار المنهج الوصفي التحليلي االستطالعي نظرا لكونه األكثر مالءمة للبحث ً الحالي، واستبانة وزعت على مجتمع ال
... Show MoreMixed ligand metal complexes of CrIII, FeIII,II, NiII and CuII have been synthesized using 5-chlorosalicylic acid (5-CSA) as a primary ligand and L-Valine (L-Val) as secondary ligand. The metal complexes have been characterized by elemental analysis, electrical conductance, magnetic susceptibility measurements and spectral studies. The electrical conductance studies of the complexes indicate their electrolytic nature. Magnetic susceptibility measurements revealed paramagnetic nature of the all complexes. Bonding of the metal ion through –OHand –COOgroups of bidentate to the 5-chlorosalicylic acid and through –NH2 and –COOgroups of bidentate to the L-valine by FT-IR studies . The agar diffusion method has been used to study the antib
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