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Novel azo ligand based on tryptamine, and its metal complexes with antioxidant properties were synthesized through chemical methods and characterized through various techniques, including IR, Mass, UV-Vis spectroscopy, elemental analysis, conductivity, magnetic sensitivity, and
thermogravimetric analysis. According to the IR spectra of the complexes, the azo-ligand, [5-(2-(3H-
1-indol-3-yl) ethyl) diazenyl) quinolin-8-ol] coordinates with metal ions through the nitrogen atom
in the quinoline ring and the oxygen atom of the hydroxyl group. Thermal analysis techniques were
employed to investigate the thermal behavior of the compounds. The results revealed that the metal
complexes possess higher thermal stability compared to the free ligand. T
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