يهتم هذا البحث بتحضير وتشخيص ليكاند ثنائي السن -: [4-(5,5-dimethyl-3-oxocyclohex-1-enylamino)-N-(5-methylisoxazol-3-yl)benzene sulfonamide] [H2L] وذلك من صهر السلفاميثوكسازول مع الدايميدون بدرجة ºC)140 (ُ ولمدة نصف ساعة , حظر معقد الكوبالت مѧن تفاعѧل هѧذا الليكاند مع ايون الكوبالѧت الثنѧائي وبطريقѧة التصѧعيد الا ُ رجѧاعي باسѧتعمال الايثѧانول وسѧطا للتفاعѧل . شѧخص الليكانѧد والمعقѧد المحضر باستعمال الطرائق الطيفية التي اثبتت ان المعقد ذات شكل هندسѧي ربѧاعي السѧطوح حѧول الايѧون المركѧزي . كمѧا تѧم ايجاد نسبة أتحاد الفلز بالليكاند المحضر (L:M (باستعمال طريقتي النسبة المولية والتغيرات المستمرة وكانѧت النسѧبة (1:1) . دُرست الظروف المثلى لازالة معقد الكوبالت من خلال الامتزاز على سѧطح البنتونايѧت وكѧذلك دراسѧة المتغيѧرات المѧؤثرة فѧي عملية الامتزاز وهي زمن الاتزان ودرجة الحرارة وقѧيم pH ووزن المѧادة المѧازة وحجѧم دقѧائق المѧادة المѧـازة . وقѧد أظهѧـرت النـتائـج ان الزمـن اللازم للوصـول الى اتـزان التـركيز هو min) 60 (. بينما النمط العام لايزوثيرمات الامتزاز هو مـن نѧوع (1L (وفق تصنيف جيلز . وقد حسبت قيم الدوال الثرموديناميكية (ΔG , ΔH ,ΔS (وفسرت النتائج في ضوئها .
The wear behavior of alumina particulate reinforced A332 aluminium alloy composites produced by a stir casting process technique were investigated. A pin-on-disc type apparatus was employed for determining the sliding wear rate in composite samples at different grain size (1 µm, 12µm, 50 nm) and different weight percentage (0.05-0.1-0.5-1) wt% of alumina respectively. Mechanical properties characterization which strongly depends on microstructure properties of reinforcement revealed that the presence of ( nano , micro) alumina particulates lead to simultaneous increase in hardness, ultimate tensile stress (UTS), wear resistances. The results revealed that UTS, Hardness, Wear resistances increases with the increase in the percentage of
... Show MoreContemporary art has been widely affected by technology, and ceramics production is no exception. As an ancient art that originates from clay and other humble materials found in the ground, ceramics is considered one of the most adaptable art forms. Once it is realised how flexible ceramics as a material is, it can be easily altered into endless forms and shapes. Therefore, it is vital for ceramics practitioners to find a relationship between this wonderful material and the media of contemporary art, culture and modelling software or technology in general so that they can take their deformable art pieces to a whole new level. Such a relationship is worth investigating. Thus, for the purposes of this research, several ceramic pieces were
... Show MoreIn this work an experimental simulation is made to predict the performance of steady-state natural heat convection along heated finned vertical base plate to ambient air with different inclination angles and configurations of fin array. Two types of fin arrays namely vertical fins array and V-fins array on heated vertical base plate are used with different heights and spaces. The influence of inclination angle of the plate , configuration of fins array and fin geometrical parameters such as fin height and fin spacing on the temperature distribution, base convection heat transfer coefficient and average Nusselt number have been plotted and discussed. The experimental data are correlated to a formula between average Nusselt number versus R
... Show Moreتكمن مشكلة البحث في أن كليات التربية عامةً وكلية التربية /ابن الهيثم خاصة ما زالت تسير وفق أنماط إدارية تقليدية وأن هناك شكوى تلهج بها الألسن في المجتمع المحيط بأن المخرجات التعليمية لا توازي تطلعات المجتمع وتوجهاته المستقبلية، كذلك الأهمية لتطبيق معايير ضمان جودة تحقق المستوى المطلوب لهذه الكلية أسوة بالمعايير العالمية، إذ هدف البحث في معرفة واقع معايير ضمان الجودة في الكلية والانتقال إلى رؤية مستقبلية ل
... Show MoreZygapophyseal joints (or facet joints), are a plane synovial joint which located between the articular facet processes of the vertebral arch which is freely guided movable joints. Ten dried vertebrae were used for the lumbar region and taking (L4) as a sample to reveal stress pathways across the joints by using ANSYS program under different loading conditions which used Finite Elements Analysis model. Results obtained from the ANSYS program are important in understanding the boundary conditions for load analysis and the points of stress concentration which explained from the anatomical point of view and linked to muscle and ligament attachments. This model used as a computational tool to joint biomechanics and to prosthetic im
... Show MoreThe study aimed to identify how to raise grateful children from an Islamic educational perspective. For that objective to be achieved, the researcher used both of deductive and descriptive approaches using the method of documentary research. The study's results show that children are the real wealth of the community and the foundation of cultural building; therefore, paying attention their raising is a responsibility that must be shared by everyone; gratitude is part parcel of the Islamic doctrine, which is one of the greatest virtues; the virtue of gratitude is the attitude of the believers which in turn strengthens the bonds and expands the network of positive social relationships; It is also considered a cultural significance
... Show MoreManufacturing industries are at the beginning of the thinking of those who put economic policies in developed countries and also more in developing countries, where manufacturing is the engine of industrial and economic development through its performance and its effective role in the formation of GDP, as well as the great advantages that characterize this sector and affect Largely on sustainable development, as well as its importance in its influential role in protecting national industry through increased exports and reduced imports.
Iraq is one of the countries that rely on its oil economy to rely entirely on the provision of needs and requirements of the state, and this
... Show Moreتسعى تركيا ضمن سياساتها المائية ومنذ زمن بعيد وبأصرار على تنفيذ المزيد من بناء السدود والمشاريع التخزينية المائية على حوضي دجلة والفرات، الامر الذي يؤدي بالضرورة الى تناقص معدل الواردات المائية لنهري دجلة والفرات الداخلة للاراضي العراقية .وبالتالي التأثير على مقومات التنمية الزراعية العربية بشكل عام والتنمية الزراعية بالعراق بشكل خاص ومن ثم تهديد الامن الغذائي الوطني.
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... Show MoreThis paper presents a sight about the chemical structure deformation of poly (ethylene-co-vinyl acetate) (EVA) samples according to the change ratio of rate constant values. Spectroscopy kinetics fluorescence curves are fitted for two characteristic wavelength domains of fluorescent intensities. The short wavelengths (320-400 nm) domain show spectra overlapping, while at long wavelengths (400-800 nm) domain spectra are arranged in regular for each specific accelerated aging time. The ratio of kinetics rate constant at long wavelengths to kinetics rate constant of short wavelengths is the criterion of the degree chemical structure deformation. Molar extrin
... Show MoreThe shoulder and hip joints though essentially both are ball and socket joints, show structural variability to serve functional needs.
This study aims at revealing some of the structural and functional properties of each of the two joints regarding the factors that contribute to the stability of any joint in the body, namely: bone, ligament, and muscle.