One of the main causes for concern is the widespread presence of pharmaceuticals in the environment, which may be harmful to living things. They are often referred to as emerging chemical pollutants in water bodies because they are either still unregulated or undergoing regulation. Pharmaceutical pollution of the environment may have detrimental effects on ecosystem viability, human health, and water quality. In this study, the amount of remaining pharmaceutical compounds in environmental waters was determined using a straightforward review. Pharmaceutical production and consumption have increased due to medical advancements, leading to concerns about their environmental impact and potential harm to living things due to their increasing presence. Many nations now acknowledge that pharmaceutical pollution of the aquatic environment poses a threat to the environment. It is quite possible that some endocrine active drugs have effects at extremely low environmental concentrations because they exhibit very high biological potencies even at Wg/day doses. Sample preparation requires a number of procedures, including the filtration and extraction of pharmaceutical environmental waters, ND IT IS is a crucial step in environmental analysis. Pre-concentrate is used to prevent extraction inefficiencies caused by suspended solids. Several analytical techniques, such as hyphenated mass spectrometry and chromatography, have been used for the identification and determination of pharmaceuticals in environmental waters. For citation: Jasim M. S. Jamur A review of analytical methods for the analysis of pharmaceuticals in environmental samples. ChemChemTech [Izv. Vyssh. Uchebn. Zaved. Khim. Khim. Tekhnol.]. 2025. V. 68. N 4. P. 20-24. DOI: 10.6060/ivkkt.20256804.7151.