This research involves an indirect Fluorophotometric method for the determination of microgram amount of oxymetazoline hydrochloride in the concentration range 0.1-5.0 g/ml. The method is based on the oxidation of the drug by cerium sulphate solution which is acidic medium where Ce IV is reduced to Ce III which can be excited at 259 nm to give an emitted light at 377 nm which is directly proportional to the concentration of Ce III which is equivalent to Ce IV that is needed to oxidize the studied drug. The average recovery of the method is 100.19% and relative standard deviation (RSD) < 0.37% . The method have been successfully applied to the determination of the studied drug in its pure and pharmaceutical preparations and it wa
... Show MoreThe potential of Euphrates poplar (EP) leaves, a plentiful agricultural waste, as a sustainable adsorbent for wastewater treatment is examined in this work. FTIR, FESEM, and XRD were used to characterize activated carbon (AC) derived from EP leaves by carbonizing them at 400°C for 3 hours. Brunauer found a surface area of 3.77 m²/g using the Brunauer–Emmett–Teller (BET) technique. Methylene blue (MB) adsorption trials showed that with an ideal contact time of 60 minutes, the removal efficiency exceeded 91%. Temperature and pH significantly affected the adsorption process, and the addition of EP nanoparticles enhanced dye uptake. According to kinetic modeling, the Temkin isotherm (R²= 0.904) provided the most accurate equilibrium f
... Show MoreTo create nanoparticles of zinc oxide (ZnO), a green chemistry method was used. Using Cordia myxa (ZnO-C) and Ziziphus spina (ZnO-Z) extracts works like natural reduction and stabilization properties. The green process provided enhanced phytochemical interactions, which facilitated nanoparticle formation and improved stability. The concentrations of Zn and O elements were validated using energy-dispersive X-ray spectroscopy. The ZnO-C and ZnO-Z polycrystalline structures with a hexagonal wurtzite phase were validated by X-ray diffraction (XRD), where the average crystalline size is about 17.54 nm for ZnO-C, while for ZnO-Z it is equal to 16.809 nm. Field emission scanning electron microscopy (FESEM) micrograph of ZnO-C
... Show MoreThe concept of cubic ideals is an important generalization in an algebraic structure. In this work, we introduce the notion of a cubic Q-sub-algebra and a cubic Q-ideal within a Q-algebra. Some properties of a cubic Q-ideal with a cubic BCK-ideal are studied, and a few results of these ideals are discussed. Such that every cubic Q-ideal is a cubic BCK-ideal, and the opposite is not true. Also, the concept of the level set of a Q-algebra as a cubic set is defined, and some important results associated with it have been shown. The relationship between a cubic Q-ideal and a Q-ideal with a cubic Q-sub-algebra and a Q-sub-algebra by the level set is proved. Finally, the image and the inverse image of cubic Q-ideals under a homomorphism are
... Show MoreThe development of technology is becoming necessary in multiple fields that specialize in human interaction life. This has contributed to increasing awareness of electronic financial transactions by enhancing the ease of handling currencies, especially by employing vending machines in commercial markets and airports. Vending machines have become widespread nowadays, and due to their ease of use for customers, it has become necessary to pay attention to this type of device. Due to the different currencies adopted in countries around the world, there has emerged a need to increase the flexibility of programming these machines to be suitable for the countries using the devices. In this research, an intelligent convolutional neural network m
... Show MoreCrypto systems deployed in smart cards and embedded devices are vulnerable to side-channel attacks, in which adversaries exploit power consumption to recover secret keys. Correlation power analysis (CPA) and machine-learning-based attacks can break AES-128 implementations with relatively few traces. This work investigates Neural Signal Obfuscation (NSO) as a practical countermeasure for an AES-128 smart card-style implementation. We first acquire and characterize power traces from the target device and quantify baseline leakage using traces-to-disclosure (TTD), guessing entropy (GE), signal-to-noise ratio (SNR), and the success rate of a neural network attacker. We then design and train a lightweight one-dimensional convolutional obfusca
... Show MoreAmlodipine Besylate (AMB) was determined in pharmaceutical and biological samples using a continuous-flow injection technique characterized by simplicity, rapidity, cost-effectiveness, sensitivity, and a broad linear range. This study aims to develop and evaluate a flow injection analysis method for the rapid and reliable determination of Amlodipine in chemical and biological samples using minute quantities. The suggested method is based on the oxidation of the drug with a potassium bromide-potassium bromate mixture, followed by reaction with crystal violet as a reagent to produce a blue product, the absorbance of which was measured at 592 nm. The coefficient of determination (R2) is 0.9978, and the calibration curve's linear range is
... Show MoreIn this study, transition complexes of Fe(III), Zn(II), La(III), Ce(III), and Pr(III) with a Schiff base ligand (L), which is derived from 3-hydroxybenzaldehyde and sulfamethoxazole, as the primary ligand, and L-Leucinate as a secondary ligand. The bonding mode of the Schiff base has been confirmed through a range of techniques, including infrared, UV-visible (UV-Vis), carbon and proton nuclear magnetic resonance spectroscopy, mass spectrometry, and elemental analysis. All complexes were characterized by elemental analysis, conductivity measurements, and spectroscopic techniques, including UV-Vis and Fourier transform infrared spectroscopy. A thorough discussion is provided on the structural and bonding features of the mixed ligand compl
... Show MoreZnTe possesses the proper optoelectronic properties as a candidate for device development. The structure and optical properties of ZnTe semiconductor thin films of 500 nm were studied using thermal evaporation technique. The influence of annealing temperatures on ZnTe thin films in the range ( R.T - 473 K). XRD and surface morphological analyses are used to examine the films. The ZnTe films are comparatively polycrystalline and cubic in phase, according to the XRD analysis. with a lattice constant of 0.61 nm upon an (111) orientation. The intensities of all the peaks rapidly increase though they show the same tendencies; it shows the crystallinity of the films becomes higher crystal size diameters (from 8.41 to 12.18nm) both increase as
... Show MoreA fracture is a damage to bone tissue that causes damage to the tissue surrounding the bone and may penetrate the skin. Subjects and methods: the present study included (80) fractured Iraqi patients (and 40) patients with DM2 and (40) without DM2 and compared them with (40) healthy control. Patients and control are matched in age. This study showed a significant increase in retinol-binding protein 4 (RBP4) and a considerable decrease in Vit .A GPT and GOT in fracture patients with and without DM2. In addition, there was a significant negative correlation between RBP4 with (GPT and GOT) in fracture patients with DM2 and a significant positive correlation between RBP4 with (GPT and GOT) in fracture patients without DM2.
... Show MoreThis study investigates new concepts in grill topological spaces by employing specified sets in which the α-open sets are defined. Many scholars, such as Choquet, who is considered the first to lay the foundation stone for the concept of a grill and formulate its definition, were interested in studying it. After that, many attempts have been made to study the properties associated with this concept and to understand the relationships among these properties. There are several types of grill topological spaces, including discrete and cofinite topologies. Properties of this set and certain relationships are studied, as well as examining a group of functions, like open, closed, and continuous functions, determining their relation with each
... Show MoreThis study presents the execution of an iterative technique suggested by Temimi and Ansari (TA) method to approximate solutions to a boundary value problem of a 4th-order nonlinear integro-differential equation (4th-ONIDE) of the type Kirchhoff which appears in the study of transverse vibration of hinged shafts. This problem is difficult to solve because there is a non-linear term under the integral sign, however, a number of authors have suggested iterative methods for solving this type of equation. The solution is obtained as a series that merges with the exact solution. Two examples are solved by TA method, the results showed that the proposed technique was effective, accurate, and reliable. Also, for greater reliability, the approxim
... Show MoreThe configurations of the nuclear shell model were employed to study and inspect the form factor of a scattering electron in the 58Ni nucleus. The wave function of the model space was obtained through the (fp-orbits) and (fpd6) effective interactions within the model space by utilizing the Harmonic Oscillator wave functions as a single particle's wave function. In the (fp-LS) shell, the correction for the main calculations of model space was performed by the 1st-order perturbation theory to estimate the effects of core polarization with the (2ℏω) energy of excitation that has been carried out. Core polarization combined the model space with the discarded space (higher configuration core)
... Show MoreTransition ion complexes have various commercial and technical uses, including antibacterial, antifungal, and anticancer medications and catalysts; their characteristics are critical regarding their kinetic impact. This study aims to synthesize new complexes, copper and nickel complexes, characterize them using spectral techniques, determine their chloride content, evaluate their anti-oxidant effect, and examine the antibacterial activity of the ligands and their complexes against gram-positive bacteria (Staphylococcus), gram-negative bacteria (Escherichia coli), and Candida albicans. All chemicals were used strictly as provided, with no additional purification; CuCl2.2H2O and Ni(
... Show MoreThe main purpose of this paper is to study a predator – prey dynamical system consisting of three species prey, specialized predator and generalist predator namely H (t), I (t) and J (t) respectively, w food web and refuge for the prey and specialized predator population. The consider system has five equilibrium points A0=(0, 0, 0), A1=(1, 0, 0), A2=(h, i, 0), A3=(h, 0, j), and the positive equilibrium point A4=(h, i, j) .The stability and bifurcation of the equilibrium points was studied and the main influence was the qualitative behavior of the solution. It was found that A0 was unstable while the other equilibrium points are stable
... Show MoreThe sol-gel method was used in this study to create the Zn-CdFe2O4/SnO2(0.15) nano ferrite, and XRD, FE-SEM, and EDX methods were used to evaluate the nano ferrite's characteristics. The findings showed that the lattice constant of the sample CdFe2O4/SnO2(0.15) is higher than that of ZnFe2O4/SnO2(0.15) and Zn0.5Cd0.5Fe2O4/SnO2(0.15) and that the resultant compound possesses a cubic spinel ferrite phase. The crystal size was on the nanoscale, according to Scherrer-Williamson Hall. Based on the FE-SEM images, it can be noticed its shape as semi-spherical or spherical; the prese
... Show MoreCrude oil is known globally as one of the major causes of environmental pollution. This chemical compound exerts exhausting impacts on cultivable lands and water surfaces, leading to profound damage to agriculture and aquatic life. Over the years, several bioremediation approaches have evolved to manage this pollution problem properly. A phylum of microorganisms known as cyanobacteria offers an efficient alternative to established bioremediation methods. We conducted the present study to investigate the effectiveness of cyanobacteria in eliminating residual total petroleum hydrocarbon (TPH). Synechococcus algae treated three concentrations of crude oil (0.6, 1.8, and 3 ppm) over four time periods (on days 3, 6, 9, and 12). The g
... Show MoreIn this paper, orthogonal polynomials and their operational matrices will be utilized to address the initial and boundary value problems of the one-dimensional wave problem, where the domain of the space variable is bounded, which covers a variety of scientific and engineering operations. Six types of orthogonal polynomials, Include instead of such as the Genocchi, Bernoulli, Legendre, Boubaker, Chebyshev and Standard polynomials. The linear problem with its initial and boundary conditions are transformed to a linear algebraic equations, which can then be solved by utilizing to get an approximate solution for this problem. Some test problems related to the one-dimensional wave equation with different conditions are discussed and solved
... Show MoreGreen synthesis of nanoparticles (NPs) has gained attention as an eco-friendly alternative to conventional methods, reducing toxicity to the environment and living organisms. This study aims to synthesize a novel nanocomposite (Mag-Chi-Cur-AgNPs) composed of silver NPs (AgNPs) prepared using curcumin (Cur) as a reducing and stabilizing agent, along with chitosan (Chit) and magnetic iron oxide (Mag). Cur-AgNPs were synthesized by dissolving Cur in dimethyl sulfoxide and deionized water, followed by the controlled addition of AgNO3. The solution was stirred, pH-adjusted, ultrasonicated, and incubated. Chit-Cur-Ag nanocomposite was formed by dissolving nanochitosan in acetic acid, mixing it with Cur-AgNPs, then stirring, washing,
... Show MoreAnastatica hierochuntica is believed to be very useful in Arab countries for treating various health disorders. The aqueous extract of Anastatica hierochuntica was investigated for its effects on hormones in mice females. the aqueous extract of plant at a dose level of 100mg/1mL showed significant increase (p<0.05) on levels of hormones LH, FSH, PRL level and PRO level. Clomid treated group showd significant increase in LH, FSH, and PRL while there was non-significant increase in PRO. From the above results, it is concluded for the first time that aqueous Anastatica hierchuntica extract offers significant effect of LH, FSH, PRL, and PRO in this mice females scompared with control.
In this work , we applied the nuclear shell model by using Modified Surface Delta Interaction ( MSDI ) to study the nuclear structure for Ti42-44 nuclei from the calculation of the energy level values and its total angular momentum . After comperation with the experiment values which found to be rather in good agreement and determined the total angular momentum values of energy levels which are not assigned experimently , as soon as , we certify some values that were not certained experimently .
The aims of the paper are to present a modified symmetric fuzzy approach to find the best workable compromise solution for quadratic fractional programming problems (QFPP) with fuzzy crisp in both the objective functions and the constraints. We introduced a modified symmetric fuzzy by proposing a procedure, that starts first by converting the quadratic fractional programming problems that exist in the objective functions to crisp numbers and then converts the linear function that exists in the constraints to crisp numbers. After that, we applied the fuzzy approach to determine the optimal solution for our quadratic fractional programming problem which is supported theoretically and practically. The computer application for the algo
... Show MoreUsing an electrochemical polymerization technique at room temperature, poly nicotine amide (PNA) was produced from the monomer nicotine amide (NA) in aqueous solution. The structure of polymer layer generated on the stainless steel surface (316 L) (working electrode) is investigated by Fourier Transmission Infrared Region (FT-IR). The anti-corrosion activity of polymer coating on the stainless steel (SS 316 L) is investigated by electrochemical polarization in 0.20M solution of HCl at 293-323K. The graphene -modified polymer film-coated SS had greater protection efficiency (PE percent) when compared to Nano ZnO -modified polymer film-coated SS. For the corrosion process of SS 316 L, kinetic and thermo-dynamic parameters of activation are
... Show MoreThe effect of SiO 2 ) Silica) on the dielectric and physical properties of Mnx-Ni1 -xFe2O4 ،، X=0.5 is studies. The samples are prepared by the conventional manufacturing
method. We found that the physical and dielectric properties of Mn-Ni ferrite change
considerably with the substituent samples .the variation of dielectric constant as a function of
frequency of ferrite system decrease with frequency increases and increase with the increase
the concentration of SiO 2 . It was found that the increase of SiO 2 concentration of all our
samples produce an increase in mass density and decrease with porosities
The com pton profiles for Ti02 have been measured using a SCi
Am-241 compton spectrometer .A pellet of the oxide was prepared from a polycrystalline powder having a thickness of 1.54 mm ,about J 00000 counts have been accumulated at the compton peak
.Theoreti cal compton profiles have been calculated for different ionic anangements using free atom compton profile for the core electrons.The theoretical and experimental results ahrce well for (Ti/4(0 .2 arrangement which support complete transfer of valence electrons from metal to oxygen ions, i.e., full ionic &nbs
... Show MoreThe ion-pair formation method has been applied for the spectrophotometric determination of Cimetidine and Erythromycin ethylsuccinate, in bulk samples and in dosage form. The methods are accurate, simple, rapid, inexpensive and sensitive depending on the extraction of the formed ion-pair with brompthymol blue (BTB) as a chromogenic reagent in chloroform, use phthalate buffer of pH 5.5 and 4.0 for Cimetidine and Erythromycin ethylsuccinate respectively. The formed complexes show absorbance maxima at 427.5 nm and 414.5 nm for Cimetidine and Erythromycin ethylsuccinate respectively against reagent blank. The calibration graphs are linear in the ranges of 0.5-15 µg.mL-1 with detection limit of 0.222 µg.mL-1 for
... Show MoreThis paper is Interested with studying the performance of statistic test the hypothesis of independence of the two variables (the hypothesis that there is no correlation between the variables under study) in the case of data to meet the requirement of normal distribution in the case away from the distribution due to the presence of outliers (contaminated values) and compared with the performance of some of the other methods proposed and modified
E. coli was isolated, and it was Gram-negative rod bacteria that was colony circular, regular edged, thick somewhat glitter and viscous(less). It was lactose fermenter bacteria and belongs the family of Enterobacteriaceae. E. coli showed sensitivity to all used antibiotics except Erythromycin (E), Cloxacellin (CX), Rifampin (RA), Cephalothin (KF), Ampicillin (AM), and Penicillin (P). The experimental results of antibiotic sensitivity of E. coli in media containing different concentrations of omeprazole, a proton pump inhibitor, showed an enhancement of resistance by decreasing the sensitivity of E. coli inversely with drug concentration against the antibiotics that E. coli was sensitive to. It seems that omeprazole changed cell mem
... Show MoreIn the present study, serum GOT(Glutamic Oxalacetic Transaminase) was purified, the purified enzyme showed the maximum activity at 37ºC and pH 7.5. During purification of serum GOT ion exchange chromatography lead to four separate forms (termed I, II, III and IV). GOT II with the highest specific activity was pure after chromatography on Sephacryl S300. . S.GOT levels were investigated in serum samples from patient with pulmonary tuberculosis .The S.GOT levels were determined at and 37ć .The study revealed that the serum GOT activity was higher in patient of tuberculous pulmonary than in control subjects.The mean serum GOT activity in the patients group was(90±8 IU/L) as compared to control group (27±0.65I
... Show MoreThe focus of this article, reviewed a generalized of contraction mapping and nonexpansive maps and recall some theorems about the existence and uniqueness of common fixed point and coincidence fixed-point for such maps under some conditions. Moreover, some schemes of different types as one-step schemes ,two-step schemes and three step schemes (Mann scheme algorithm, Ishukawa scheme algorithm, noor scheme algorithm, .scheme algorithm, scheme algorithm Modified scheme algorithm arahan scheme algorithm and others. The convergence of these schemes has been studied .On the other hands, We also reviewed the convergence, valence and stability theories of different types of near-plots in convex metric space.