Bioactivity
Mass spectroscopy
Azo complexes
Spectroscopic studies
Thermal analysis
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4-Amino-N-(5-methyl-isaxazol-3-yl)-benzenesulfonamide, a new azo
(LH) ligand, was synthesized by reacting the diazonium salt of
Sulfamethoxazole with coupling compound 3-amino phenol.
Spectroscopic techniques (UV-Vis, FTIR, 1H &13C-NMR, and LC-Mass) as
well as micro elemental analyses (C.H.N.O) and TGA and SDC were used
to identify the azo ligand. Complexes of (Zn(II), Cr(III), Cu(II) and VO(II))
were produced and characterized by atomic absorption, elemental
microanalysis, infrared, LC-Mass, TGA, DSC and UV-Vis spectral
techniques, as well as conductivity and magnetic quantifications. All the
complexes had a 1:2 metal-ligand ratio, and non-electrolytes at all
complexes and tetrahedral geometry suggested except Cr-complex, which
demonstrate
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